AOCS Official Methods — Index

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(AOAC) method (References, 1).Cd 11-57 ) may be used as an alternateH 15-52 , Procedure section.Ba 2a-38 2-Thiobarbituric Acid ValueCd 19-90 2. Ladle with handle.G 1-40 3. Automatic pipet or automatic burette.Cd 18-90 3. Glass wool.Ca 6c-65 3. Magnetic stirrer—with Teflon™-coated stirring bar.Tu 1a-64 3. Sieve—6 mesh, 30-38 cm. diameter.Ad 1-48(Applicable to sampling tung fruit or hulled tung fruit during unloading from truck, wagon or carload lots.) 5. Spatula—with 25-30 cm blade.Dd 1-59 = > = oan 3Cd 1-25 Accelerated Light Exposure of Edible Vegetable OilsCg 6-01 Acetone ToleranceTt 1a-64 Acetone-Insoluble MatterJa 4-46(Applicable to lecithin ftom soybeans and corn.) Acid ValueCd 3d-63 Acid ValueJa 6-55 Acid ValueTe 1a-64 Acid ValueTe 2a-64(“Applicable to all commercial fatty acids and polymerized fatty acids.) Acid Value of Fatty AcidsDa 14-48 Acid Value, Jojoba OilCi 4-91 Acid-Insoluble AshBa 5b-68(Applicable to oilseed meal products.) Acidity, Method AF 9a-44 Acidity, Method BF 9b-44(Applicable to sulfonated or sulfated oils except in the presence of ammonium or triethanolamine soaps or…) Acidity, Method CF 9c-44(Applicable to dark colored sulfonated or sulfated oils, except in the presence of ammonium or trietha-…) Activity of Hydrogenation CatalystsTz 1a-78 Aflatoxin StandardsAa 10-88(Standards to be used for aflatoxin quantitation (see Notes, Caution).) AflatoxinsAa 8-83(Applicable to cottonseed, cottonseed meats, cottonseed flakes, cottonseed meal, and ammoniated cotton- seed…) AflatoxinsAb 6-68(Applicable to raw and roasted peanuts, peanut meal, and peanut butter (see Notes, 1).) AflatoxinsAb 7-91(Applicable to corn, raw peanuts, and peanut butter with concentrations 210 pg/kg (ppb).) AflatoxinsAh 1-72(Applicable to copra and copra meal.) Aflatoxins in CornAj 1-86(Applicable to white and yellow corn.) Aflatoxins in CornAj 3-87(Applicable to corn.) Aflatoxins M, and M, in Dairy ProductsCb 6-86 Air OvenH 3-45 Air Oven MethodDa 2a-48 Air Oven MethodDb 1-48 Alcohol-Insoluble MatterDc 3b-59 Alcohol-Soluble and Alcohol-Insoluble MatterDa 3-48 Alcohol-Soluble and Alcohol-Insoluble MatterDb 2-48(This method is applicable to soap and soap products containing synthetic detergents.) Alcohol-Soluble MatterDc 3a-59 Alkaline SilicatesDa 18-48 Alkaline SilicatesDb 9-48(Applicable to the fatty acids of all soaps and soap products containing synthetic detergents.) AlkalinityDc 6-59 Ammonium Chlorides, Vacuum Oven MethodTc 2a-64 Analysis for Phosphorus in OilCa 20-99 Analysis of Aflatoxin Using HPLCAa 11-05(The method is applicable to the analysis of aflatoxin containing extracts when using HPLC.) Analysis of Lecithin Co-ProductsJa 12-89 Analytical Guidelines for AssessingCk 1-07 Analytical Guidelines for Testing Feed Grade Fat ProductsCf 1-68 Analytical Guidelines for the DeterminationCi 1-91 Antioxidants in Oils and FatsCg 7-05 Antioxidants—Liquid Chromatographic MethodCe 6-86 AOCS serial procedureCd 10-57 APPARTUSBc 1-50(‘Applicable to sampling soybean flour during production or at storage or transit points,) Appendix Primary Standard Preparation/Gravimetric ProcedureTf 5-91 Applicable to all normal fatty acids (see Notes, 1).Tg 1a-64 Applicable to all vegetable lecithins.Ja 14-91 Applicable to cottonseed (see Notes, 1).Aa 1-38(Applicable to cottonseed (see Notes, 1).) Applicable to cottonseed linters and cottonseed hull fibers.Bb 1-38(Applicable to cottonseed linters and cottonseed hull fibers.) Applicable to flaxseed (see Notes, 2).Af 1-54(Applicable to flaxseed (see Notes, 2).) Applicable to refined glycerin.Ea 9-65 Applicable to so: “ats and waxes.Cc 10b-25 Applicable to soybeans.Ac 1-45(Applicable to soybeans.) Applicable to sunflower seed.Ai 1-80(Applicable to sunflower seed.) AshBa 5a-49(Applicable to cake and meal from cottonseed, soybeans, peanuts, and flaxseed.) AshBe 5-49(Applicable to high-fat, low-fat, and defatted soybean or canola flours.) AshCa 11-55 AshTm 1a-64 Ash of Fatty Quaternary Ammonium ChloridesTm 2a-64 Ash-Gravimetric MethodF 2c-44 Assessing Oil Quality and StabilityCg 3-91 Atomic Absorption Spectrophotometry UsingCa 18-79 Biodiesel by the QTA® System MethodCk 2-09 Bleaching TestCc 8a-52 Bleaching TestCc 8b-52(Applicable to refined cottonseed oil.) BoraxDa 17-52(Applicable to the fatty acids of all soaps and soap products.) Bound MCPD and GlycidolCd 29b-13 Brookfield ViscosityJa 10-87 Butyric AcidCa 5c-87 Butyric AcidCa 5e-13 Calculated Saponification ValueCd 3a-94 Calibration of Rheological InstrumentsCj 3-99 Carbonates, Gravimetric Absorption MethodDa 19a-42 Carbonates, Volumetric Evolution MethodDa 19b-42 Cellulose Yield Pressure-Cook MethodBb 3-47(Applicable to cottonseed linters and cottonseed hull fiber.) ChloridesDa 9-48 ChloridesDb 7-48(Applicable to soap and soap products containing synthetic detergents.) Chlorides, Modified Wijs MethodTg 3a-64 Chlorophyll PigmentsCc 13-55 Chlorophyll PigmentsCh 4-91 Cloud Point TestCc 6-25 Cold TestCc 11-53 Collaborative Study ProceduresM 4-86 ColorCc 13a-43 ColorCc 13b-45 ColorCc 13e-92 ColorCc 13j-97 ColorTd 1a-64(Applicable to fatty quaternary ammonium chlorides.) Color after HeatingTd 3a-64 Color Spectrophotometric MethodCc 13c-50 Color, Photometric IndexTd 2a-64(Applicable to industrial oils and derivatives with light colors, such as certain fatty nitrogen compounds.) Color, Platinum-Cobalt ScaleTd 1b-64 Colorimetric Determination of PhosphorusCa 12a-02 Column Gas ChromatographyCh 2a-94 Combined AlcoholsDc 5-59 Combined Sodium and Potassium OxidesDa 27-48 Combustion Method for DeterminationBa 4f-00(This method is applicable for the determination of crude protein in soybean meal (References, 1, 3).) Commercial HexaneH 16-56 Congeal PointCc 14-59 Consistency Penetrometer MethodCc 16-60 Continue extraction for 4 hr.H 2-41 CopperDa 31-58(Applicable to soap powders.) Corn and Corn-Based Food by LiquidAj 5-93(Applicable to corn and corn products, and may be used in the analysis of corn meal and breakfast cereals.) Corn and Peanuts by Thin-LayerAa 9a-97(Applicable to corn and raw peanuts.) Cottonseed, Meats, Collets, and Extracted MealsBa 7b-96(Applicable to full-fat cottonseed, cottonseed meats, or expanded collets and solvent-extracted cottonseed…) Cottonseed, Peanuts, and Peanut ButterAj 6-95(Applicable to screening aflatoxin B,, B,, and G, contamination in whole cottonseed and peanut butter at 220…) Crude Fatty AcidsCa 5b-71 Crude FiberBa 6-84(Applicable to grains, meals, flours, feeds, and all fiber-bearing material from which the oil or fat can be…) Crude Fiber Analysis in Feeds by Filter Bag TechniqueBa 6a-05(This method is applicable to all feed materials such as grains, meals, pet foods, mixed feeds, forages, and…) Crude Fiber in Soybean FloursBc 6-49(Applicable to high-fat, low-fat, and defatted soybean flours.) Crude Vegetable OilsCc 13i-96 Cyclohexane MethodCd 1b-87 Detection and Quantification of CocoaCe 11a-07 Detection of a Volatile Organic Contaminant by GC-MSCa 3c-01(This method is suitable for identification of the following compound classes: saturated halogenated hydrocar-…) Detection of Cottonseed Oil Halphen TestCb 1-25 Detection of Non-Cocoa Butter Vegetable FatsCe 10-02 Detection of Sesame OilCb 2-40(Kapok oil reacts with an intensity equal to or greater than that of cottonseed oil, and fats from animals…) Detection of Teaseed Oil Fitelson TestCb 3-39(Applicable to normal animal and vegetable fats and oils.) Detection of Triglyceride Adulteration of Jojoba OilCi 2-91 Determination of (+)-, (-)-, and Total GossypolBa 8a-99(Applicable to decorticated cottonseed, cottonseed meats, and ground extracted meal samples.) Determination of Alkalinity in Fats and OilsCd 3e-02 Determination of B-Carotene in MargarineCe 9-01 Determination of Benzo(a)pyrene in Edible Oils and FatsCd 21-91 Determination of Cadmium ContentCa 18d-01 Determination of Chlorophyll Content in Rapeseed/CanolaAk 2-92(‘This method specifies a spectrometric method for the determination of the chlorophyll content of rapeseed…) Determination of cis-, trans-, Saturated, MonounsaturatedCe 1h-05 Determination of Cocoa Butter EquivalentsCe 11-05 Determination of Copper, Iron, and NickelCa 18b-91 Determination of Crude Glycerin, Titrimetric MethodEa 6-94 Determination of Dimethylpolysiloxanes in Fats and OilsCd 24-95 Determination of Fatty Acids in Edible OilsCe 1a-13 Determination of Fatty Acids in the 2-PositionCh 3-91 Determination of Fumonisins B1, B2, and B3 in Corn by Liquid ChromatographyAj 5a-97(Applicable for determination of total fumonisin B,, B,, and B, in corn at 800-12,800 ng/g.) Determination of Impurities in OilseedsAm 4-02(This method determines the impurities content in oilseeds used as primary industrial materials.) Determination of Lead by Direct Graphite Furnace AASCa 18c-91 Determination of Lecithin Phospholipids by HPLCJa 7b-91 Determination of Lecithin Phospholipids by HPLC-LSDJa 7c-07 Determination of lodine Value by Pre-calibrated FT-NIRCd 1e-01 Determination of Mass per Unit VolumeCc 10c-95(Applicable to so: “ats and waxes.) Determination of Mono- and DiglyceridesCd 11b-91 Determination of Oil Content in OilseedsAm 2-93 Determination of Oil, Moisture and VolatileAm 1-92(Determinations may be made either on the cleaned seed or on the sample as received (cleaned seed plus…) Determination of Polar Compounds in Frying FatsCd 20-91 Determination of Polymerized TriglyceridesCd 22-91 Determination of Saturated, cis-Monounsaturated, and cis-Polyunsaturated Fatty AcidsCe 1i-07 Determination of Sediment in Crude FatsCa 3d-02(This method determines sediment that can be separated from crude fats and oils by centrifugal force.) Determination of SodiumDd 5-92 Determination of Specific Extinction of OilsCh 5-91 Determination of the Relative Density 20/20 in AirEa 7-95 Determination of Tocopherols in Lecithin by HPLCJa 13-91(This procedure is applicable to the following co-products related to lecithin manufacture: deodorizer distil-…) Determination of Trace Elements in OilCa 17-01 Determination of Visible Foots in Crude Fats and OilsCa 3e-02(This method specifies a method for the determination in crude fats or oils of visible matter which can be…) Determination of Wax Content by CapillaryCh 8-02 Dicarboxylic Acid Composition by Gas-LiquidTy 1a-76 Diene ValueTh 1a-64 Direct Methylation of Lipids in Foods by Acid-Alkali HydrolysisCe 2c-11 Direct Methylation of Lipids in Foods by Alkali HydrolysisCe 2b-11 Dowtherm A™ by HPLCCd 25a-00 Dropping PointCc 18-80 DSC Melting Properties of Fats and OilsCj 1-94 Essential Fatty Acids (EFA)Cd 15-78 Ester SulfitesDc 4-59(Applicable to the determination of alcohol-insoluble matter in all fatty alkyl sulfates.) Evaluation of Bleaching Clays and AdsorbentsCc 8f-91(Applicable to soybean oil.) Extraction-Titration MethodF 2b-44 Fats and Oils by Gas ChromatographyCg 4-94 Fats by HPLCCe 8-89 Fatty Acid Composition by Packed Column Gas ChromatographyCe 1-62 Fatty Acid Composition of Marine Oils by GLCCe 1b-89 Fatty Acids in Marine and Other OilsCe 11-07 Fatty MatterDb 10-48 Fatty Quaternary Ammonium ChloridesTe 3a-64(Applicable to all neutral and synthetic drying oils, epoxidized oils, fatty alcohols, and fatty esters.) Fatty-acid-bound 3-MCPD and GlycidolCd 29c-13 Flash and Fire Points, Cleveland Open Cup MethodTn 1a-64 Flash Point Closed Cup MethodCc 9b-55 Flash Point of Fatty Quaternary AmmoniumTn 2a-86 Flavor Panel Evaluation of Vegetable OilsCg 2-83 Flavor Scores of Edible OilsCg 1-83 Forced Draft OvenH 1-39(Applicable to all acidulated soap stocks, regardless of type.) Foreign Matter in Laboratory SampleAa 2-38(Application to laboratory sample of cottonseed (sce Notes, 1).) Free Acid or Free AlkaliDa 4a-48(Applicable to soap and soap products.) Free Acid or Free AlkaliDb 3-48(Applicable to all soap and soap products containing synthetic detergents.) Free Alkali and Potassium CarbonateDa 5-44 Free Fatty AcidsAa 6-38(Applicable to cottonseed oil extracted according to method Aa 4-38 or oils obtained from dehulled and ground…) Free Fatty AcidsAb 5-49(Applicable to peanuts.) Free Fatty AcidsAc 5-41(Applicable to soybeans.) Free Fatty AcidsAe 4-52(Applicable to castor seeds (see Notes, Caution).) Free Fatty AcidsCa 5a-40 Free Fatty Acids in Crude Vegetable OilsCa 5d-01 Free GlycerolDa 23-56 Free GossypolBa 7-58(Application to cottonseed, cottonseed meats, cottonseed slab and sized cake, and cottonseed meals of normal…) Gardner ColorJa 9-87 GENERAL SAMPLING PROCEDURETa 1e-70 Generic Combustion Method for Determination of Crude ProteinBa 4e-93(This generic method is applicable to determine crude protein in animal feeds, oilseed meals and oilseeds…) Glycerol, Sodium Periodate Oxidation MethodEa 6-51 Glycidol Fatty Acid Esters in Edible OilsCd 29a-13 Grind the sample in a Wiley millBa 1-38 Heat Transfer Fluids in Oils—Dowtherm™ by GCCd 25-96 Hexane Residues in Fats and OilsCa 3b-87(This method is applicable to the determination of “free” volatile hydrocarbons, expressed in terms of hexane,…) Hexane-Insoluble MatterJa 3-87 Hot Plate MethodF 1b-44 Hydroxyl ValueCd 13-60 Hydroxyl Value of Epoxidized OilsTx 1a-66 Identification of OilsCb 4-35 Ifa method is from another organization, citation mustM 1-92 Indicator MethodTf 1b-64 Individual Triglycerides in Oils and Fats by HPLCCe 5c-93 Industrial TolueneH 19-58 Inorganic SaltsF 6-44 Insoluble ImpuritiesCa 3a-46(Applicable to all normal fats and oils.) International.Aj 6a-97(Applicable to screening aflatoxin B,, B,, and G, contamination in corn at 220 ng/g.) Iodine ValueCd 1-87(Applicable to fatty quaternary ammonium chlorides.) Iodine Value, Wijs MethodDa 15-48(Applicable to fatty or rosin acids after separation from soap.) Iodine Value, Wijs MethodTg 1-64 Iron and Nickel in Vegetable OilsCa 15-75 ISO 5508Ch 2-91 ISO 6799-; COICh 6-91 Isolated trans Isomers Infrared Spectrometric MethodCd 14-95 Isopropyl AlcoholH 18-58 Laboratory SampleDa 1-45 Laboratory SampleDc 1-59 Low-Resolution Nuclear MagneticCd 16b-93 Melting Point Capillary-Tube MethodCc 1-25 Methods for Testing Polymerized Fatty AcidsS 5-64 Modified Bleach Test for Soybean OilCc 8e-63 Modified Wijs MethodTg 2a-64 MoistureJa 2a-46 MOISTURETa 1-09 Moisture and Volatile MatterAa 3-38(Applicable to cottonseed.) Moisture and Volatile MatterAb 2-49(Applicable to peanuts, whole nuts and shelled stock.) Moisture and Volatile MatterAc 2-41(Applicable to soybeans.) Moisture and Volatile MatterAd 2-52(Applicable to tung fruit, hulled tung fruit, hulls and mixtures of hulled tung fruit and hulls.) Moisture and Volatile MatterAe 2-52(Applicable to castor seeds (see Notes, Caution).) Moisture and Volatile MatterAf 2-54(Applicable to flaxseed.) Moisture and Volatile MatterAi 2-75 Moisture and Volatile MatterBa 2b-82(Applicable to oilseed protein concentrates.) Moisture and Volatile MatterBc 2-49(Applicable to high-fat, low-fat, and defatted soybean flours.) Moisture and Volatile MatterBd 2-52(Applicable to castor pomace (see Notes, Caution).) Moisture and Volatile MatterCa 2b-38(Applicable to all of the ordinary fats and oils, including emulsions, such as butter, oleomargarine, and…) Moisture and Volatile Matter Air Oven MethodCa 2c-25(Applicable to animal and vegetable fats, but not to drying or semidrying oils or oils of the coconut group.) Moisture and Volatile Matter Fatty Acids Hot Plate MethodTb 1a-64(Applicable to dibasic acids in pourable solid form, during production, or at storage in various types of…) Moisture and Volatile Matter Vacuum Oven MethodCa 2d-25 Moisture by Distillation MethodDc 2-59 Moisture by the Distillation MethodDd 2a-59 Moisture Contents of Oilseeds Using PulsedAk 4-95(This method applies to rapeseed with a moisture content of less than 10%, For seeds with higher moisture…) Moisture Distillation MethodCa 2a-45(This method is applicable to all normal fats and oils, including emulsions, for the determination of mois-…) Moisture Karl Fischer ReagentCa 2e-84(Applicable to fats and oils that do not react with, and are soluble in, the reagents and that do not contain…) Moisture, Distillation MethodDa 2b-42(This method is applicable to soaps and soap products.) Moisture, Distillation MethodF 1a-44 Moisture, Karl Fischer ReagentJa 2b-87 Moisture, Karl Fischer Volumetric MethodEa 8-58 Mono- and Diglycerides Determination by HPLC-ELSDCd 11d-96 Near Infrared Spectroscopy InstrumentAm 1a-09(This procedure presents general tools for the management of near infrared (NIR) instruments, the develop-…) Negative Second Derivative InfraredCd 14e-09 Neutral OilG 5-40 Neutral Oil (Unsulfonated Material)Dd 4-60 Neutral Oil and LossCa 9f-57 Nitrogen Solubility Index (NSI)Ba 11-65(Applicable to ground soybeans, whole or ground full-fat and defatted soy flours and grits, and soybean meal.) Nitrogen-Ammonia-ProteinAc 4-91(Applicable to soybeans.) Nitrogen-Ammonia-ProteinBa 4a-38(Applicable to cottonseed meats, and meal and ground cake or pellets from cottonseed, soybeans, peanuts and…) Nitrogen-Ammonia-ProteinBa 4d-90(Applicable to cottonseed meats, and meal and ground cake or pellets from cottonseed, soybeans, peanuts, and…) Nitrogen-Ammonia-ProteinAa 5-91 Nitrogen-Ammonia-ProteinBc 4-91(Applicable to high-fat, low-fat, and defatted soybean and canola flours.) Nitrogen-Ammonia-Protein Modified Kjeldahl MethodAb 4-91(Applicable to peanuts (groundnuts).) Nitrogen-Ammonia-Protein Modified Kjeldahl MethodAi 4-91(Applicable to sunflower seed.) NONVOLATILES (SOLIDS)Tu 1a—64(Fatty quaternary ammonium chlorides are defined as industrial products containing essentially R,R,R,R,NCI,…) OilAb 3-49(Applicable to raw and roasted peanut kernels (see Notes, 1).) OilAc 3-44(Applicable to soybeans.) OilAd 3-52(Applicable to whole tung fruit.) OilAd 5-52(Applicable to tung kernels.) OilAd 6-52(Applicable to hulled tung fruit.) OilAe 3-52(Applicable to castor seeds (see Notes, Caution).) OilAg 1-65(Applicable to safflower seed.) OilBa 3-38(Applicable to cottonseed meats, and cake and meal from cottonseed, soybeans, peanuts, and flaxseed.) OilBb 2-38(Applicable to cottonseed hulls.) OilBc 3-49(Applicable to high-fat, low-fat, and defatted soybean flours.) OilBd 3-52(Applicable to castor pomace (see Notes, Caution).) Oil ContentAi 3-75 Oil ContentAf 3-54(Applicable to flaxseed.) Oil Content of Oilseeds by Nuclear Magnetic ResonanceAk 3-94(“Applicable to rapeseed, soybean, sunflower seed, and peanut.) Oil in Corn GermAj 4-89(This method is applicable to whole kernel corn or its milled component parts (see Notes, 1).) Oil in Oilseeds: Supercritical Fluid Extraction MethodAm 3-96(This two-part method is specifically designed to determine either (a) process-scale extractable oil with…) Oil Stability IndexCd 12b-92 Olive and Olive-Pomace OilsCh 7-09 Oven Storage Test for Accelerated Aging of OilsCg 5-97(These Analytical Guidelines list the application of procedures for testing and measuring the quality and sta-…) Oxirane OxygenCd 9-57 Pensky-Martens Closed Cup Flash TesterCc 9c-95(Applicable to animal, vegetable, and marine fats and oils.) Percent Non-Amines in Fatty Amines and DiaminesTw 1a-64 Peroxide ValueJa 8-87 Peroxide Value Acetic Acid-Isooctane MethodCd 8b-90 pH of Acidulated Soap StocksG 7-56 PhosphatesDa 20a-48 PhosphatesDa 20b-57 Phospholipids in Vegetable Oils Nephelometric MethodCa 19-86 PhosphorusCa 12-55(Applicable to animal fats and vegetable and marine oils.) Phosphorus by Direct Graphite FurnaceCa 12b-92 Physical Analysis of Tung FruitAd 4-52(“Applicable ro whole tung fruit.) Polyethylene in Fats and OilsCa 16-75 Polyunsaturated AcidsCd 7-58 Potentiometric Determination of ChloridesDb 7b-55(Applicable to all soaps and soap products containing synthetic detergents.) Preparation of Methyl Esters of Long-Chain Fatty AcidsCh 1-91 Previous AOCS versions of iodine value methods specifiedCd 1d-92 Primary Amine Composition By Gas ChromatographyTf 4a-77(Applicable to materials containing only fatty primary amines, difatty secondary amines, trifatty tertiary…) Primary, Secondary and Tertiary Amine ValuesTf 2b-64 Primary, Secondary, and Tertiary Amine ValuesTf 2a-64(Applicable to fatty amines.) Protein Dispersibility Index (PD!)Ba 10b-09(Applicable to ground soybeans, whole or ground full-fat or extracted flakes, full-fat and defatted soy flours…) Protein Dispersibility Index (PDI)Ba 10-65(Applicable to ground soybeans, whole or ground full-fat or extracted flakes, full-fat and defatted soy flours…) Protein Dispersibility Index (PDI)Ba 10a-05(Applicable to ground soybeans, whole or ground full-fat or extracted flakes, full-fat and defatted soy flours…) Purity by Total Acidity and Acid Value, Dibasic AcidsTe 4a-70 Quantification of Free Glycerin in SelectedCa 14b-96 Quaternary Ammonium ChloridesTv 1a-64(Applicable to fatty quaternary ammonium chlorides.) Rapeseed and Canola by HPLCAk 1-92(This method does not determine glucosinolates that are substituted on the glucose molecule, but these…) Rapid Determination of Isolated trans Geometric IsomersCd 14d-99 Rapid Determination of Oil/Fat UtilizingAm 5-04(This method is applicable to extractions of oilseeds (see Numbered Notes, 1), meats, feeds, and foods and is…) Reference 4) or ISO 5509Ce 2-66(The method is applicable to methyl esters of fatty acids having 8-24 carbon atoms and to animal fats,…) Refined and Bleached ColorCc 8d-55(Applicable to refined soybean oil and refined sunflower oil.) Refined and Bleached Color and Saponification ColorCc 13f-94 Refining LossCa 9a-52 Refractive IndexCc 7-25(Applicable to all normal animal and vegetable fats.) Refractive IndexTp 12-64 Reichert-Meiss!, Polenske and Kirschner ValuesCd 5-40 Residual LintAa 7-55(Applicable to cottonseed.) Rosin Acids in Fatty AcidsTs 1a-64 Rosin, McNicoll MethodDb 11-48(Applicable to soaps containing synthetic detergents.) SamplingAb 1-49(Applicable to peanuts, whole nuts and shelled stock.) SamplingC 1-47(Applicable to the sampling of animal and vegetable fats, and crude and refined vegetable and marine oils.) SamplingEa 1-38 Saponification ColorCc 13g-94 Saponification ColorCc 13h-94(Applicable to high-quality tallows and coconut oils.) Saponification ValueCd 3-25 Saponification ValueCd 3b-76(The saponification value is calculated from the normalized fatty acid composition determined by gas-liquid…) Saponification ValueDa 16-48 Saponification ValueDb 8-48 Saponification Value Modified Method Using MethanolCd 3c-91 Screen TestBe 7-51(Applicable to high-fat, low-fat, and defatted and reconstituted soybean flours.) Screen TestDa 28-39 Selectivity of Hydrogenation CatalystsTz 1b-79 Separation and Analysis of OrganophosphorusCd 23-93 Simultaneous Determination of OilAk 5-01(The method wires the following st r ple into the magnetic field of a pulsed rs) Slip Melting Point AOCS Standard Open Tube Melting PointCc 3-25(Applicable to all normal animal and vegetable fats.) Slip Melting Point ISO StandardCc 3b-92 Smoke, Flash and Fire PointsCc 9a-48 Soap in Oil Titrimetric MethodCc 17-95 Sodium Alkylbenzene Sulfonate by Ultraviolet AbsorptionDd 3-60 Sodium and Calcium by Atomic Absorption SpectrophotometryCa 15b-87 Sodium SulfateDe 7-59 Solid Fat Content (SFC)Cd 16-81 Solutions of Drying Oils, Hot Plate MethodTc 1a-64 SPECIFIC GRAVITYTp 1a-64(This method covers the selection and application of procedures for testing commercial fatty acids from…) Specific GravityTo 1b-64 Specific GravityTo 1a-64 Spectrophotometric DeterminationCc 13k-13 Spectrophotometric Determination of Conjugated Dienoic AcidTi 1a-64 SpreadabilityCj 4-00 Standard Hydrochloric Acid SolutionH 14-52 Standard Sodium Hydroxide SolutionH 12-52 Standard Sulfuric Acid SolutionH 13-52 Standard Test SievesH 20-11 Starch, Munson, and Walker MethodDa 25-48 Steroidal Hydrocarbons in Vegetable OilsCd 27-96 Sterols in Soy Sludges and ResiduesCe 3-74 Stigmastadienes in Vegetable OilsCd 26-96 Sugars, Munson and Walker MethodDa 24-48 SulfatesDa 22-48 Surplus Status of MethodsM 3-82 Synthetic Methyl AlcoholH 17-58 Test AOCS MethodTf 3a-64(Fatty amines are defined as industrial products containing essentially RNH,, R,NH, and R,N, where R is a…) Tetrasodium PyrophosphateDa 21-48 The following values for reproducCa 6a-40 The temperature of the fatty acidsDa 12-48 Thermal Heating Fluids in Vegetable OilsCd 25b-07 Thermometer SpecificationsH 5-40 Thin-Layer ChromatographyJa 7-86(Applicable to all vegetable lecithins.) TI 12-64TI 12-64(Applicable to vegetable oil deodorizer distillates and sludges.) TI 1a-64TI 1a-64(Applicable to all normal fats and oils (see Notes, 1).) Titer TestCc 12-59(Applicable to all normal, refined and dry animal and vegetable oils.) Titer TestDa 13-48 Titer TestG 6-40(Applicable to all types of soapstock.) Titer TestTr 1a-64 Titration MethodF 2a-44(This method is applicable to sulfonated and sulfated oils that do not contain mineral acids, free sulfonic…) TLC Confirmation of AflatoxinsAa 9-86(Applicable to solutions suitable for TLC of cereal grains, cottonseed, and peanuts, and their products.) Total Active IngredientsF 4-44(Applicable to sulfated oils, but not to test samples that are not completely decomposed upon boiling with…) Total Alkalinity of Alcohol-Insoluble MatterDa 7-48(Applicable to soaps and soap products.) Total Alkalinity of Alcohol-Insoluble MatterDb 5-48(Applicable to all soaps and soap products containing synthetic detergents.) Total Amine Value of Fatty Amines, Potentiometric MethodTf 1a-64 Total AmmoniaF 8-44 Total Anhydrous SoapDb 6-48(Applicable to all soda soaps and soda soap produ of the alcohol-insoluble matter, expressed as Na,O or…) Total Anhydrous Soap and Combined AlkaliDa 8-48(Applicable to soda soaps and soda soap products.) Total Desulfated Fatty MatterF 3-44 Total Fatty AcidsG 4-40 Total GossypolBa 8-78(Applicable to decorticated, glanded and glandless cottonseed, cottonseed flour, cooked cottonseed meats, cot-…) Total Gossypol in OilsCa 13-56 Total Hexane Content in Extracted MealsBa 14-87(This method is applicable to the determination of the total amount of volatile hydrocarbons, expressed in…) Total Tocopherols in Deodorizer DistillateCe 7-87 Total, Free and Combined GlycerolCa 14-56 trans Fatty Acids by Silver-Ion Exchange HPLCCe 1g-96 Triglycerides by Gas ChromatographyCe 5-86 Triglycerides in Vegetable Oils by HPLCCe 5b-89 Trypsin Inhibitor ActivityBa 12-75(Applicable to soybean meals and flours (raw and toasted), to soy protein concentrates and isolates, and to…) Unsaponifiable MaterialTk 1a-64 Unsaponifiable MatterCa 6b-53 Unsaponifiable MatterDa 11-42(Applicable to all soap and soap products.) Unsaponifiable Nonvolatile MatterF 5-44 Unsulfated MaterialDc 8-59(Applicable to fatty alkyl sulfate free from added alkaline builder.) Urease ActivityBa 9-58(Applicable to soybean meals, soy flour and to soybean mill feeds, except when urea has been added.) Vacuum OvenH 4-45 Viscosity of Transparent LiquidsTq 12-64(Applicable to drying oils and all fatty acids.) Viscosity of Transparent Liquids by Bubble Time MethodJa 11-87(Applicable to lecithin products that are fluid at the specified temperature.) Volatile HydrocarbonsDa 26-42(Applicable to all soaps and soap products.) Volatile Matter in Fats and OilsCa 2f-93(Applicable to crude fats and oils.) Water-Immiscible Organic SolventsF 10-44(Applicable to sulfonated or sulfated oils in the presence of ammonium ot triethanolamine soaps, or both.) Water-Insoluble MatterDa 6-48(Applicable to potash paste soaps.) Water-Insoluble MatterDb 4-48 Wet Extraction MethodG 3-53(Applicable to raw and acidulated soapstock from all types of fats and oils.) Wijs SolutionCd 6-38 Writing and Approval of MethodsM 2-09 X-Ray Diffraction Analysis of FatsCj 2-95 Zearalenone and a-Zearalenol in CornAj 2-86(Applicable to corn.) “Free” Hexane Content in Extracted MealsBa 13-87(This method is applicable to the determination of “free” volatile hydrocarbons, expressed in terms of hexane,…)